O-methoxybenzaldehyde

Kufotokozera Kwachidule:

Kuchokera ku salicylaldehyde ndi methylation reaction ndi dimethyl sulfate.Sakanizani 3kg ya sodium hydroxide mu 30% yankho lamadzi, onjezerani 12.2kg ya salicylaldehyde ndi 80L yamadzi poyambitsa, ndi kutentha mpaka kuwira.Pang'onopang'ono yonjezerani 12.9kg ya dimethyl sulfate, sungani yankho la reflux kwa pafupifupi 3h mutawonjezera, pitirizani reflux kwa 2-3h kutsatira Chemicalbook ...


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Dzina lachi China:o-methoxybenzaldehyde

Dzina lina:o-methoxybenzaldehyde;2-methoxybenzaldehyde;2-anisaldehyde;o-anisaldehyde;o-methoxybenzaldehyde;salicaldehyde methyl ether;o-anisaldehyde;salicylaldehyde methyl ether

Molecular formula:C8H8O2

Kulemera kwa mamolekyu:136.15

Manambala System

Nambala ya CAS:135-02-4

EINECS:205-171-7

HS kodi:29124900

Magawo aukadaulo

Maonekedwe: kristalo wopanda mtundu wa prismatic

Chiyero: ≥98.0%

Malo osungunuka: 39°C

Malo otentha: 238°C, 70-75°C/0.2kPa

Kachulukidwe wachibale: 1.1326 (20/4°C)

1.5597

Pothirira: 117°C

Kusungunuka: kusungunuka mu mowa, ether, benzene, osasungunuka m'madzi

Njira Yopangira

Kuchokera ku salicylaldehyde ndi methylation reaction ndi dimethyl sulfate.Sakanizani 3kg ya sodium hydroxide mu 30% yankho lamadzi, onjezerani 12.2kg ya salicylaldehyde ndi 80L yamadzi poyambitsa, ndi kutentha mpaka kuwira.Pang'onopang'ono onjezani 12.9kg wa dimethyl sulfate, sungani yankho la refluxed kwa pafupifupi 3h mutatha kuwonjezera, pitirizani reflux kwa 2-3h kutsatira Chemicalbook, kuziziritsa wosanjikiza mafuta, kusamba ndi 5% sodium hydroxide solution, ndiyeno kusamba ndi madzi pH 8. , kuwonjezera Anhydrous potaziyamu carbonate ndi zouma.Pambuyo pochotsa desiccant, distillation pansi pa kupanikizika kochepa, kusonkhanitsa distillate pa 120 ° C (2.0kPa), yomwe ndi o-methoxybenzaldehyde.The methylation reaction amathanso kuchitidwa mu zosungunulira toluene, ndi zokolola za 60%.

Cholinga

Methoxybenzaldehyde ndi yapakatikati mu kaphatikizidwe ka organic, yomwe imagwiritsidwa ntchito popanga zonunkhira ndi mankhwala.O-methoxybenformaldehyde angagwiritsidwe ntchito popanga.O-Methoxybenzaldehyde angagwiritsidwe ntchito kupanga adrenergic mankhwala Chuankening.


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